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Current Analytical Chemistry - Online First
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51 - 63 of 63 results
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Acoustic-assisted Fabrication, Characterization, and Photocatalytic Application of Ni2O3/NiO/rGO Nanocomposites
Authors: Islam Gomaa, Fatama Gamal, Maryam G. Elmahgary, Medhat A. Ibrahim and Nasser Mohammed HosnyAvailable online: 10 October 2024More LessIntroduction This study introduces an innovative two-step approach to fabricate a high-performance Ni2O3/NiO/rGO nanocomposite photocatalyst. The process synergistically combines solvothermal precursor synthesis with calcination and high-energy ultrasonic irradiation, enabling the in-situ formation of a thin Ni2O3 layer on NiO quasi-sphere nanoparticles anchored to a reduced graphene oxide (rGO) matrix. Method The inc Read More
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Fabrication of Surface-Enhanced Raman Scattering (SERS) Substrates in Analytical Science by Natural-inspired Materials: A Review
Authors: Kai Li, Lan Zhang, Le Wang, Liqiang Guo and Yajing LiAvailable online: 09 October 2024More LessSurface-Enhanced Raman Scattering (SERS) spectroscopy, as a novel rapid detection technology, offers molecular fingerprinting capabilities that achieve trace-level detection. The key to optimizing SERS sensitivity and reliability lies in the precise control of the nanostructures of SERS substrates. Nature, through billions of years of evolution, has served as a masterful creator, developing organisms with remarkable abili Read More
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Carbon-based Nanocomposite Materials for Electrochemical Monitoring of Cadmium Ions
Authors: Manorama Singh, Dev Kumari Patel, Smita R. Bhardiya and Rahul KumarAvailable online: 09 October 2024More LessIn the present era of science and technology, cadmium poisoning in humans is reported from several parts of the world and now it is a global health problem. Accumulation of cadmium in human organs and tissues, such as the liver, kidney, etc., leads to carcinogenic effects and toxicity to the organ system. Therefore, several efforts are being made to develop a monitoring system for cadmium metal ions in the environmen Read More
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A Review of Analytical Methods for Microplastics in Soils
Authors: Yuting Liu and Jiafu LiAvailable online: 08 October 2024More LessMicroplastics (MPs), as an emerging environmental pollutant, pose a potential threat to ecosystems and human health, and the study of their analytical methods has become particularly important. In this paper, the current research progress of analytical methods for MPs in soil is reviewed. The sources, ecological impacts and possible health risks of MPs are introduced, and the urgency of accurate detection and q Read More
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Study of Physical Mechanical Characteristics, Economic Viability, and Carbon Emission Impacts of Recycled Aggregate
Authors: Zheyuan Feng, Zhibo Zhang, Pengwei Li, Yu Zhou and Cheng ChenAvailable online: 08 October 2024More LessIntroduction Construction and Demolition Waste (CDW) constitutes a major portion of solid waste and presents a significant environmental challenge. This study aims to evaluate the transformation of CDW into a Recycled Aggregate (RA) as a sustainable strategy to mitigate environmental pollution. Method The research assesses the mechanical properties and economic benefits of RA concrete, which is mad Read More
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Electrochemical Determination of Tartrazine and Carmoisine Dyes from Aqueous Solutions on Modified Electrodes
Authors: Shaista Jabeen, Shah Bano and Safeer AhmedAvailable online: 08 October 2024More LessIntroduction The recognition of the health hazards of azo dyes has highlighted the need to develop efficient, rapid, and reliable analytical methods for dye determination. Method In this work, electrochemical probing of the azo group of Tartrazine (TZ) and Carmoisine (CR) in food dyes was carried out. Synthesized bismuth and zinc oxide nanoparticles were used to modify Graphite Electrode (GE). Results Electrochemical ana Read More
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Chitosan–sodium Tripolyphosphate–CuO Biopolymer–nanocomposite as an Efficient Electrocatalyst for Water Splitting
Authors: Angel Grace Raja, Kalai Arasi Selva Arasu and Rajakumari RajaramAvailable online: 08 October 2024More LessBackground Fossil fuels have been used extensively as primary energy sources, which has resulted in nearly depleted reserves, a contaminated environment, and a variety of negative health effects globally. Hydrogen has been proposed by researchers as an effective “carbon neutral” fuel. Large-scale hydrogen production through electrochemical water splitting necessitates the use of inexpensive, extremely effective, and e Read More
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A Review on Advancement in Analytical Quality by Design (AQbD)
Authors: Ankit Kumar Singh, Yogita Vashitha, Ashita Jain, Ghanshyam Das Gupta and Sant Kumar VermaAvailable online: 07 October 2024More LessAnalytical Quality by Design (AQbD) represents a transformative methodology in pharmaceutical development, anchored in a systematic, risk-based, and data-driven framework. This approach optimizes analytical methods, fostering heightened product quality, efficient regulatory compliance, and informed decision-making. The industry's increasing acceptance of AQbD principles signifies a paradigm shift towards e Read More
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Enzymeless Gabapentin Sensor Based on Prussian Blue-modified Indium Tin Oxide Electrodes for Sensing Gabapentin in Capsules
Authors: Wael Alshitari and Waleed A. El-SaidAvailable online: 07 October 2024More LessBackground In this study, we reported on developing a susceptible, accurate, simple, and economical electrochemical sensor for gabapentin determination in capsules. Methods The ITO electrode was modified with a layer of Prussian blue nanoparticles and then used as the working electrode. Gabapentin was extracted from commercial capsules, and a series of concentrations of gabapentin were prepared for studyi Read More
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Novel Chiral HPLC Method for Accurate Identification and Quantification of RS Enantiomers in Ropivacaine on Immobilized Chiral Stationary Phase: Development and Validation
Available online: 04 October 2024More LessPurpose Ropivacaine is a widely used local anesthetic for managing postoperative pain, particularly in procedures such as caesarean sections. While historically used as a racemate, its structural similarity to mepivacaine and bupivacaine within the pipecoloxylidide group is notable. Both enantiomers of ropivacaine exhibit similar nerve-blocking properties, but the R enantiomer is associated with increased cardiotoxicity co Read More
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Investigation of Voltametric Behavior and Antioxidant Activity of Vanillin-based Chalcone Compound
Available online: 02 October 2024More LessBackground Chalcone-type molecules are significant compounds due to their biocompatible properties. This study aimed to examine the electrochemical properties of vanillin chalcone monomer (VC) and its polymer (PANI-VC), as well as to investigate the antioxidant properties of the vanillin chalcone monomer. Methods VC and PANI-VC were synthesized and characterized using FTIR and UV-Vis spectroscopy. The elect Read More
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An Efficient and Cost-effective Modified Carbon Paste Electrodes for Diltiazem Hydrochloride Determination in Tablets
Available online: 02 September 2024More LessBackground and Objective This study presented new sensitive and selective modified carbon paste (MCPE) potentiometric sensors modified with different ion pairs for the determination of the antihypertensive drug diltiazem hydrochloride (DTM-HCl) in biological fluids, pharmaceutical preparations, and in its pure form. Methods Plasticizers, ion pair type, ion pair content, response time, temperature, and pH were just a Read More
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Progress in the Development of Antifouling Electrochemical Biosensors
Authors: Liuxing Chen, Da Chen and Meiling LianAvailable online: 02 September 2024More LessElectrochemical biosensors a subclass of biosensors, consisting of a biosensing element and an electrochemical transducer, have been widely used in various fields due to their excellent performance and portable device. However, in complex actual samples, non-specific adsorption of proteins and solid particles, and adhesion of cells and bacteria will lead to problems such as reduced sensor sensitivity, prolonged response time, Read More
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