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- Volume 9, Issue 2, 2022
Current Microwave Chemistry - Volume 9, Issue 2, 2022
Volume 9, Issue 2, 2022
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Microwave-Assisted Flow Chemistry for Green Synthesis and Other Applications
Authors: Tara Mooney, Maysa Ilamanova and Béla TörökUsing combined microwave-assisted flow chemistry approaches is one of the most active areas of microwave chemistry and green synthesis. Microwave-assisted organic synthesis (MAOS) has contributed significantly to developing green synthetic methods, while flow chemistry applications are quite popular in industrial chemistry. The combination of the two has farreaching advantages. In early studies, the flow chemistry co Read More
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Study on Microwave-assisted Reduction of Pyrolusite
Authors: Dongjie Liu, Jinjia Du, Qingqing Dai and Junwen ZhouManganese is a vital metal resource, and increased consumption of manganese is leading to the shortage of high-grade manganese ore resources. However, a large number of low-grade manganese ore resources ((Mn<30%) accounts for about 60% of the total manganese resources) have not been effectively utilized because of the lack of efficient industrial utilization methods. Researching new technologies for reducing low-gra Read More
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Microwave-Accelerated Facile Synthesis of pyrano[2,3-d]pyrimidine Derivatives via one-pot Strategy Executed by Agro-Waste Extract as a Greener Solvent Media
Authors: Krishnappa B. Badiger, Santosh Y. Khatavi and Kantharaju KamannaBackground: A variety of methods have been reported for the synthesis of pyrano[2,3- d]pyrimidines in the literature with some limitations, and generally used expensive catalysts, harmful solvent and prolonged reaction time. This paper describes an efficient and rapid multicomponent synthesis of pyrano[2,3-d]pyrimidine through condensation of aromatic aldehyde, malononitrile and barbituric acid catalysed by agro-w Read More
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Microwave-Assisted: An Efficient Aqueous Suzuki-Miyaura Cross- Coupling Reaction of the Substituted 1H-1,2,3-Triazoles
Authors: Satya K. Avula, Najeeb Ur Rehman, Rene Csuk, Biswanath Das and Ahmed Al-HarrasiBackground: A variety of natural products reveal the presence of the 1H-1,2,3-triazole moiety in their chemical structures. In general, these molecules also play a significant role in the agrochemical, medicinal and pharmaceutical industries. Microwave-assisted reactions have attracted great interest for researchers to synthesize 1H-1,2,3-triazole compounds in shorter times with increased yields. Objective: The objective Read More
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Microwave Assisted Synthesis of a Novel Schiff Base Scaffolds of Pyrazole Nuclei: Green Synthetic Method
Authors: Dipanjan Karati, K.R. Mahadik and Dileep KumarAim: The research aims to develop a sustainable microwave-assisted scheme for Synthesizing 5-(benzylidene amino)-1-phenyl-1H-pyrazole-4-carbonitrile congeners. Background: 5-(benzylideneamino)-1-phenyl-1H-pyrazole-4-carbonitrile scaffolds are novel molecules having various pharmacological activities such as neurodegenerative, anti-microbial, anticancer. Schiff base congeners are considered as efficient phar Read More
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Conventional vs. Microwave-assisted Synthesis: A Comparative Study on The Synthesis of Tri-substituted imidazoles
Authors: Tanvi Goel, Deepali Bansode and Naman V. JainBackground: The organic and peptide synthesis, various nanotechnology, and biochemistry processes are being carried out using microwave irradiation. The use of microwaves for synthesis has increased in the past two decades. The microwave offers several advantages such as ease of handling, lesser reaction times, quality of the product, and eco-friendly, which is green. The conventional method of synthesis, on the ot Read More
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Effect of Synthesis Conditions on the Catalytic Performances of CuO/Al2O3 in Microwave-enhanced Fenton-like System
Authors: Menghan Cao, Ke Tian, Fengyin Shi and Guangshan ZhangBackground: In previous work, we successfully prepared CuO/Al2O3 catalysts and evaluated their catalytic activity, kinetics and degradation mechanism for Fenton-like oxidation of p-nitrophenol (PNP) under microwave irradiation. However, we did not study the effect of important preparation parameters on the activities of catalysts. Objectives: (1) The effect of preparation conditions: CuSO4 concentration of the i Read More
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